SEE A ROSEMARY
EXTRACTION HERE
more extractions coming !
FAQ
Is a
Tamisium Extractor dangerous?
Any flammable solvent
extractor is potentially dangerous. No matter if it is
acetone, alcohol used in a soxhlet extractor with a heat
source or butane in a cold tamisium extractor or a
typical fuel pump extracting gas at any gas station..
Laboratory safety precautions are the same with this
extractor as with most others. The key point to note is
that the Tamisium Butane Extractors are totally closed
systems. The butane is never exposed to the air during
the normal extraction or the normal recovery process.
The apparatus is a closed system and as long as the
system is closed, you should not have any issues to deal
with. Due to the fact that no pumps or heat is needed to
extract or recover the solvent you will not have to deal
with boiling solvent fumes and sparks or flames to
ignite a solvent if an accident should occur. These
extractors are not sold to be used in non lab
environments. They are sold to be used in laboratory
settings by laboratory professionals and professional
chemist in lab or home research. The manual is very
descriptive and is almost a book guide into a new area
of extraction. A mini course in itself.
Do I need a permit to operate a
laboratory or Tamisium Extractor?
I am not aware of other states that require
permits for laboratory apparatus. Texas is one of the
only states I know of that did require a permit.
This varies in each State.
In Texas, I am required to have a permit for my other
lab equipment and an additional permit for sale of
various lab apparatus. This extractor has not been
around long enough to be listed on the Controlled
Laboratory Apparatus List for the State of Texas.. This
may change and I assume it will. I have notified TXDPS
that I invented it, use it and now sell it. I have been
asked to submit Texas State Purchase Records for all
purchases made in this state. I have agreed to this
request due to the fact that the apparatus is being
reviewed for the purpose of adding it to the Texas
Controlled Apparatus List and will most likely be added.
Be aware that upon adding it to the list, you will be
required to get a permit. I will update the site when I
hear of any changes.
I am not sure if you will be grandfathered in if your
purchase was prior to it being added or not but all
Texas Record of Purchase will be available to TXDPS from
the very first sale. I know Texas customers will be
required to gain permit if it is added to the list prior
to purchasing.
The bottom line is if you are not doing anything wrong,
you have nothing to hide. The point of a permit is for
the safety of the people in the area you live in and to
ensure that you do not get tempted to violate that
safety in regard to unlawful drug production. If
required and not obtained you will be breaking the law
in Texas for sure.
I respect you rights to privacy but in the state of
Texas I will comply with TXDPS as much as required. I am
not required to submit records for purchases in other
states unless I am contacted and requested to do so to
aid an investigation as is any other lab equipment
supplier.
It is up to the end consumer to obtain the proper
licenses and permits in the state or country they reside
in. Contact your local Dept of Public Safety or your
State Health and Safety agency for more information. In
Texas contact 512-424-2481 and ask for Jeanne Malone.
You will be pleasantly surprised at how very helpful and
encouraging Jeanne Malone and the State of Texas can be.
I am sure the same goes for any State Agency.
Is Butane
safe to use for consumable products?
Absolutely. Butane is non
toxic and evaporates completely. It has been used for
over 100 years for exactly that reason. You can use it
to extract topical and internal medicine, perfumes and
oils. Especially oils. It is the holy grail of organic
solvents and really shines with aromatic fragrances and
oils. Butane is the only solvent that will extract the
aromatic and total essence of some flowers such as Lily
of the Nile.
Is Butane
harmful or toxic?
Butane is non toxic and evaporates completely after
extraction. It boils at 32 degrees F and will rapidly
evaporate after being exposed to 80F room temperature.
What is the polarity of butane?
Butane (C4H10) has no
polar groups.
Butane is NON POLAR all the way, which means you can use
Butane as the only solvent if the chemical you want to
extract is non polar as well. If not, then you will have
to add another solvent to the butane before extracting.
Solvent amounts are determined by the saturation level
of a particular plant component in a given solvent.
Butane is composed only of carbon and hydrogen. It is
nonpolar. It has no net ionic charge.
Polar molecules can dissolve polar molecules and
nonpolar molecules can dissolve nonpolar molecules, but
they don't mix well together and will separate into two
layers in a separatory funnel. The closer you can get
the polarity to match up, the more efficient the
extraction process will be and the lower volume of
solvent that will be required. If you want to separate
them during the cleaning process, you will need the
polarity to be opposite.
Is Butane
the only solvent needed for a complete extraction?
Sometimes, to perform a complete extraction of an herb
or plant, you will need a small amount of one or more
other solvents such as alcohol or acetone. This is to be
added to the butane before you begin the extraction
process. This is the remarkable feature of using butane.
Because you can add these other solvents in a variety of
combinations, the possible plants you can extract from
is virtually unlimited. And you can extract several
chemicals from the same plant in one extraction or
isolate the extraction to one chemical in most cases.
How do you know which
solvents to use if butane is not the one required?
Solvent choice is determined by two factors.
Chemical Saturation Point, of a chemical in a given
solvent, and Chemical Polarity Matching of the solvent
to the chemical being extracted. In a 3 volume
extraction it is advisable to use 3 times the saturation
point. If 25 ml of solvent will dissolve all the
chemical in the the amount of plant material being
extracted, you should use 75 ml or more in your
extraction. If making a 4 volume extraction or 5 volume
extraction, you will need to increase the saturation
rate to 4 or 5 times respectively.
Visualize this - The column of plant material fills with
solvent, then drains and fills again and drains and
fills again and drains. This is a 3 volume extraction.
Each time the column fills and drains is considered one
volume. All the solvent required to dissolve all the
chemical or oil in that material will need to be in that
first volume because the following volumes will be only
used to wash that first volume out. In the extraction
business, we consider that 3rd volume to be the one that
gets all the extract out. To be true, the first volume
has be be able to dissolve all that you want to get out
of that plant. Otherwise the next volumes are not
washing, they are still dissolving. Remember that when
adding the primary extracting solvent to the carrier
solvent, it will be divided equally into those volumes
of carrier solvent. Hence the reason you need to add 3
times the amount required if using 3 volumes of carrier
solvent. 4 for 4 and 5 for 5 etc.
Chemical Saturation point is the point
at which a solvent will no longer dissolve a chemical.
You will need to know how much chemical resides in the
plant you are extracting from and you will need to know
how much solvent is required to dissolve all that
chemical to extract it from the plant. You will want to
double that volume of the solvent or quadruple it if
possible.
Because you are using 3 volumes of solvent to every
volume of plant material, you will need to make sure
enough solvent is in the first volume that passed
through the plant material because the 2 other volumes
are just to wash out what has already been dissolved.
Solvent Chemical Polarity matching is
something you will just have to figure out with each
plant material you extract from or look in an index or
reference source such as a Merck index or type in
polarity and name of chemical on the internet and find
it there. You can also determine from more more
mainstream extractions what is currently being used.
How efficient is butane as
a solvent?
After we built our first original prototype, before
placing any plant material inside the unit, we performed
an extraction to clean it out .. Using 99% pure butane
during the extraction process, we extracted over 200
grams of oil from the pores of the the stainless steel
extractor alone.
Why
is Butane considered such a great solvent?
You do not need
high volumes of solvents to extract when using butane as
the carrier solvent. And when used as the primary
solvent, such as is the case in most oil extractions,
the extraction process really works well due to the fact
that you are sending almost 5 volumes of butane through
the plant material when only a 1/2 of a volume would be
more than enough.
This allows for an extremely efficient extraction.
During testing, I have not been able to get one more
drop of oil out when making a second pass with clean
recovered solvent, extracting from the same extracted
plant material.
But most
important is the fact that Butane boils at 32 degrees
Fahrenheit, it is non toxic and evaporates completely
with minimal effort. The other primary solvent as well
as the extracted out chemicals boil at much higher
temperatures and will not evaporate with the butane.
This allows you to separate the several chemicals very
easily which is what makes using BUTANE as a carrier
solvent so incredible. But when it can be used as the
carrier solvent and the primary solvent as one, it
really shines. When used as the primary solvent alone,
be sure and add some solvent like alcohol in the bottom
tank. Otherwise you may be left with a goo when all the
butane has evaporated away during the recovery process.
And remember, you can use other solvents as the sole
primary solvent. But recovering them takes way more
time. But it can be done. And in some states, such as
California, where the use of butane is not allowed, it
is required to use other solvents as the sole solvent or
in combination with other allowed solvents.
In oil
extractions when using butane, how can I get all the
butane out as the oil thickens.
There should be no butane in the extract if you
recovered the butane properly. Adding a transport
solvent before beginning extraction, should assist in
the recovery of all the butane. Assuming you need to
clean the extract, adding the cleaning solvent should be
all that is needed to remove any butane should any be
left behind after recovery of the butane solvent.
Warming it up is another alternative. It will not need
to be warmed more than 110F. Never use an open flame or
heating element. Immerse the holding tank in warmed
water to warm the solvent.
Normal recovery removes all of the butane if a transport
solvent is used and the recovery time is slightly
increased. You may have some vapor pressure that resides
in the tank, and it will be expelled when opening. Use a
Safety Purge Line
to purge away remaining vapor pressure.
As more question come in, more questions and answers
will be posted.
Please use the forum to post question if possible
And email me when you do.